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X-Pulse 90 continues the X-Pulse ethos of modularity, versatility, and upgradeability, and as such can be tailored to your needs, for example, with a flow cell to monitor real-time reactions, or the addition of variable temperature capability. Additionally, the unique, user exchangeable probe enables the setup to be easily changed depending on the requirements (e.g. highest signal to noise (SNR) performance versus multiple nuclei), as well as ease of access for cleaning.
X-Pulse’s unique features that will benefit your workflow:
Click the hotspots below to explore X-Pulse 90:
Autosampler
X-Pulse 90 can be upgraded to include a 25 position auto-sampler, X-Auto. X-Auto enables automated data collection and provides a step change in productivity.
User Exchangeable Probes
As the only benchtop NMR spectrometer to offer user exchangeable probes, X-Pulse 90 is easy to maintain and has the versatility of being able to select a probe for your applications.
Flow Cell
X-Pulse 90 equipped with a flow cell makes real time reaction control and mechanistic studies straightforward. The orientation of the X-Pulse 90 diffusion gradient will ensure accurate measurement, even whilst the sample is flowing, and the excellent stability of X-Pulse 90 ensures the only variation you will see in the spectrum comes from the reaction itself.
Versatile Configuration
Configure your X-Pulse with a variety of nuclei detectable.
Broadband – ¹H/¹⁹F/ Fully tuneable ²⁹Si – ³¹P
Dual-X – ¹H/¹⁹F/ Choose two nuclei from the broadband frequency range.
Variable Temperature
Combine the high sensitivity, X-Pulse 90 with the widest variable temperature (VT) range (0-60°C) available for a benchtop NMR spectrometer. This allows a comprehensive understanding of reaction kinetics, as well as enabling users to observe a wider range of reactions. The large temperature range also facilitates investigation of the behaviour of mixtures at different temperatures.
Software
Our data acquisition software, SpinFlow, is extremely versatile. It allows users to:
X-Pulse 90 is the world's only 90 MHz broadband benchtop NMR system. X-Pulse 90 enables you to tune between a wide range of nuclei in a single benchtop instrument.
Accessories:
X-Pulse 90 Dual-X benchtop NMR system allows the analysis of up to 4 NMR active nuclei in a single instrument.
Accessories:
X-Pulse 90 HF is a single channel benchtop NMR instrument with exceptional sensitivity single channel benchtop NMR system.
Accessories:
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Benchtop NMR is a spectroscopic technique that provides structural and quantitative insights into liquid chemical samples. The minimal sample prep and non-invasive, non-destructive nature make it perfect for complementing any existing analysis techniques. Benchtop NMR can easily be brought to the lab, and when coupled with a flow cell and X-Pulse broadband capabilities, provide real time monitoring of many nuclei within a sample. To speed up analysis, X-Pulse 90 can be fitted with a 25 position autosampler allowing ‘hands free’ analysis that reduces time spent in front of the instrument and maximises instrument use.
The broadband channel on X-Pulse 90 is freely tuneable from ²⁹Si to ³¹P. This capability makes X-Pulse the most versatile benchtop NMR spectrometer available, and means you can select the nuclei suitable for your research. For example. ¹H, ¹³C, ⁷Li for battery applications; ²⁹Si for polymers; or more exotic nuclei such as ⁵⁵Mn, ⁵⁹Co or ¹⁹⁵Pt for catalysis or inorganic synthesis.
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With a magnetic field of 90 MHz (2.1 T), X-Pulse 90 allows users to separate challenging peak overlaps and positively identify compounds of interest in samples. The increased spectral dispersion means that a peak that is hard to distinguish with a lower magnetic field is now separated and easily identifiable. The increased sensitivity of X-Pulse 90 also enables detection and accurate measurement of molecules with a lower concentration, such as mass limited samples or when dealing with active pharmaceutical ingredients (APIs). The increased sensitivity and peak separation also enable much faster 2D experiments, even on larger molecules.
Our acquisition software, SpinFlow, is easy-to-use and suitable for all levels of operators from experts to infrequent users.
- Walk up and collect 1D and 2D NMR data with one click and pre-set experiments
- Set your own parameters and save experiments
- Create and save experiment queues for consistent data acquisition
- Write and execute your own pulse sequences with full control of the whole spectrometer in a Python® - based language
